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Materials ScienceContactsResearchPublicationsBeamline DescriptionSpecificationsInformation for UsersManualsSafety

Manuals

Laboratory overview

Beamline
End station including manuals in PDF PDF

Operating the beamline

Pumping and pressure reading

Opening and closing
Setting the beam position
Setting the photon energy
Setting the photon energy resolution

Operating the end station

Pumping and pressure reading
Sample mounting, transfer and manipulation
Ion sputtering
Sample cooling and annealing
Exposing the sample with gases

Quadrupole mass spectrometer

Using evaporators:

Differentially pumped ports
Knudsen-cell evaporators
E-beam evaporators
Quartz crystal microbalance
Estimated deposition rates

Using electron analyzer:

Sample alignment with respect to the analyzer and photon beam
Photoemission with X-ray source
Photoemission with synchrotron radiation (EDC)
Photoemission with synchrotron radiation (NEXAFS, RPES)

Photoemission with synchrotron radiation (ARPES, XPD)

Venting, bake-out and degassing

Control software – basic/advanced

Beamline (beamline and monochromator operation)

SpecsLab2 (XPS)
KolXPD

KolXPD (NEXAFS)

LEED Acquire (LEED)

Sample Alignment (with camera on the analyzer)

Annealing Control

Pressure Display

Quadstar (QMS)

CompactConnect (pyrometers)

Other equipment

DC power supplies and picoampermeter
Turbopumping stations
Glove bag and nitrogen gas line
Pyrometers
UV lamp
Water cooling circuit
Spot welder
Balance
Chemical lab

Troubleshooting

BCS (valve control) communication problem
Insufficient beamline water cooling
Monochromator blocked or miscalibrated
Electron analyzer connection problems
Transfer rod bayonet misaligned

At the end of the day (checklist)

Ultima modifica il Giovedì, 09 Marzo 2023 10:08

Elettra-Sincrotrone Trieste S.C.p.A. di interesse nazionale
Strada Statale 14 - km 163,5 in AREA Science Park
34149 Basovizza, Trieste ITALY
Tel. +39 040 37581 - Fax. +39 040 9380902
Anagrafe Nazionale Ricerche Cod. 51779CRP
partita IVA 00697920320